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  • Sessions listed November 29 – December 2 will be held in-person in Boston.
  • Sessions listed December 6 – 8 will be offered virtually.
  • Sessions listed as available on-demand will be available on our virtual platform November 24 – January 15.

MRS is making frequent changes to the program, which is updated daily. Please check back for updates. Presenters: please refer to official email correspondence from MRS Meetings to confirm your presentation date and time.  Please contact meetings@mrs.org if there are discrepancies.

Symposium CH01—In Situ and Operando Techniques Applied to Electrochemical Systems—A Key Toolkit for Deep Understanding

2021-11-29   Show All Abstracts

Symposium Organizers

Claire Villevieille, CEA
Kristina Edstrom, Uppsala University
Christian Masquelier, Université de Picardie Jules Verne
Y. Shirley Meng, University of California, San Diego
Tutorial CH01: Electrochemical Impedance Spectroscopy Applied to Interfacial Battery Investigation
Session Chairs
Sylvain Franger
Fabio La Mantia
Claire Villevieille
Monday AM, November 29, 2021
Virtual

8:30 AM -
Electrochemical Impedance Spectroscopy (EIS) Applied to Battery Characterization

Sylvain Franger1

Université Paris-Saclay1

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10:00 AM - CH01.00
BREAK


10:15 AM -
Dynamic Impedance Spectroscopy for Operando Battery Materials Characterization

Fabio La Mantia1

Universität Bremen1

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2021-11-30   Show All Abstracts

Symposium Organizers

Claire Villevieille, CEA
Kristina Edstrom, Uppsala University
Christian Masquelier, Université de Picardie Jules Verne
Y. Shirley Meng, University of California, San Diego
CH01.01: Cathode Materials Investigation
Session Chairs
Joshua Gallaway
Brett Lucht
Tuesday AM, November 30, 2021
Hynes, Level 3, Room 304

10:30 AM - *CH01.01.01
Nanostructure Formation as a Signature of Oxygen Redox in Li-Rich Cathodes

Karena Chapman1,Antonin Grenier1,Gabrielle Kamm1,Y. Shirley Meng2,Yixuan Li2,Hyeseung Chung2

Stony Brook University1,University of California, San Diego2

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11:00 AM - CH01.01.02
Regeneration of Degraded Li-rich Layered Oxide Materials Through Heat Treatment-Induced Transition Metal Reordering

Yixuan Li1,Mateusz Zuba2,Shuang Bai1,Zachary Lebens-Higgins2,Bao Qiu3,Zhaoping Liu3,Minghao Zhang1,Louis Piper2,Y. Shirley Meng1

University of California, San Diego1,Binghamton University2,Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences3

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11:15 AM - CH01.01.04
Late News: Established and Emerging Methodologies for Operando X-Ray Total Scattering and Pair Distribution Function Analysis for Rechargeable Batteries

Martin Karlsen1,Simon Billinge2,3,Dorthe Ravnsbæk1

University of Southern Denmark1,Columbia University2,Brookhaven National Laboratory3

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11:30 AM - CH01.01.05
Operando Single Particle Diffraction of Nax[Ni1/3Mn2/3]O2

Jason Huang1,Daniel Weinstock1,Hayley Hirsch2,Ryan Bouck1,Oleg Gorobtsov1,Malia Okamura3,Ross Harder4,Wonsuk Cha4,Jacob Ruff1,Y. Shirley Meng2,Andrej Singer1

Cornell University1,University of California, San Diego2,Carnegie Mellon University3,Argonne National Laboratory4

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11:45 AM - CH01.01.06
The Impact of Alkali-Ion Intercalation on Redox Chemistry and Mechanical Deformations—Case Study on Intercalation of Li, Na and K Ions into FePO4 Cathode

Omer Capraz1,Bertan Ozdogru1

Oklahoma State University1

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CH01.02: Electrolyte Characterization
Session Chairs
Karena Chapman
Tuesday PM, November 30, 2021
Hynes, Level 3, Room 304

1:30 PM - *CH01.02.01
Electrolyte Oxidation and the Role of Acidic Fluorophosphates in Capacity Loss for Lithium–Ion Batteries

Brett Lucht1

University of Rhode Island1

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2:00 PM - CH01.02.02
In Operando Visualization and Data-Driven Modeling of Ion Transport in Electrolytes for Lithium Metal Batteries

Yuan Yang1

Columbia University1

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2:15 PM - CH01.02.03
Operando AFM and Electrochemical Characterization of the Growth of the Solid Electrolyte Interphase

Harry Thaman1,2,Che-Ning Yeh1,Justin Rose1,William C. Chueh1

Stanford University1,SLAC National Accelerator Laboratory2

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2:30 PM - CH01.02.04
In Situ Characterization of Solid Liquid Interface by Infrared Nanospectroscopy

Xiao Zhao1,2,Yi-Hsien Lu1,Miquel Salmeron1,2

Lawrence Berkeley National Laboratory1,University of California, Berkeley2

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2:45 PM - CH01.02.05
Energy Dispersive X-Ray Diffraction (EDXRD) as a Synchrotron Technique for Spatially-Resolved Operando Study of Buried Materials and Interfaces Within Batteries

Joshua Gallaway1

Northeastern University1

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3:00 PM - CH01.02.06
In Situ and Operando Characterization of Capacity and Efficiency Limiting Phenomena in Electrochemical Energy Storage Systems

Amy Marschilok1,2,Esther Takeuchi1,2,Kenneth Takeuchi1,2

Stony Brook University1,Brookhaven National Laboratory2

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CH01.03: Imaging Techniques
Session Chairs
Raphaele Clement
Tuesday PM, November 30, 2021
Hynes, Level 3, Room 304

4:00 PM - *CH01.03.01
Looking into Key Components for Next Generation Batteries with Operando X-Ray Tomography

Aleksandar Matic1,Matthew Sadd1,Shizhao Xiong1

Chalmers University of Technology1

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4:30 PM - CH01.03.02
Unveiling the Relation Between Electrochemical Performance and Nanostructure of Fuel Cell Electrode Materials via Scanning SAXS and Ptychographic X-Ray Nanotomography

Christian Appel1,Katharina Jeschonek2,Kai Brunnengräber2,Bastian J.M. Etzold2,Marianne Liebi3,4,Manuel Guizar-Sicairos1

Paul Scherrer Institute1,Technische Universität Darmstadt2,Empa–Swiss Federal Laboratories for Materials Science and Technology3,Chalmers University of Technology4

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4:45 PM -
Open Discussion


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5:00 PM - CH01.03.04
In Situ XANES of Non-Stoichiometric Vanadium Oxide During Electrochemical Cycling of Aqueous Zn-Ion Battery

Christopher Patridge1

D'youville College1

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5:15 PM - CH01.03.05
Multimodal Study of Dis-Sodiation Mechanisms Within Individual Na3V2(PO4)2F3 Cathode Crystals Using 4D-STEM-ASTAR and STXM-XANES

Nicolas Folastre1,2,Kirill Cherednichenko1,2,François Cadiou1,Matthieu Bugnet3,4,Quentin Ramasse3,Edgar Rauch5,Jacob Olchowka6,Christian Masquelier1,2,7,Laurence Croguennec2,6,7,Arnaud Demortiere1,2

Laboratoire de Réactivité et de Chimie des Solides (LRCS) – CNRS UMR 7314/Université de Picardie Jules Verne1,Réseau sur le Stockage Electrochimique de l’Energie (RS2E) – CNRS FR 34592,SuperSTEM, SciTech Daresbury Science and Innovation Campus – University of Leeds3,MATEIS Laboratory – CNRS UMR 5510/University of Lyon4,Laboratoire Science et Ingénierie des Matériaux et Procédés (SIMaP) – Grenoble INP/CNRS/UJF5,Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB) – CNRS/Université de Bordeaux6,ALISTORE-ERI – CNRS FR 31047

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5:30 PM - CH01.03.06
Late News: Ion-Gated Transistors as In Operando Diagnosis Tools for Battery Electrode Materials

Jose Herrera1,Federico Poli2,Francesca Soavi2,Clara Santato1

Polytechnique Montréal1,Università di Bologna2

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5:45 PM - CH01.03.07
Kelvin Probe Force Microscopy Provides New Insights into Electrochemical Reactions via Suspended Graphene

Irit Rosenhek Goldian1,Salma Khatun1,Sidney Cohen1,Sa'ar Shor Peled1,Robert Weatherup2,Baran Eren1

Weizmann Institute of Science1,University of Oxford2

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CH01.04: Poster Session I
Session Chairs
Tuesday PM, November 30, 2021
Hynes, Level 1, Hall B

8:00 PM - CH01.04.02
Li Deposition in a Highly Concentrated Electrolyte Studied by In Situ Neutron Reflectometry

Josef Rizell1,Anton Zubayer2,Matthew Sadd1,Filippa Lundin1,Nataliia Mozhzhukhina1,Alexei Vorobiev3,4,Shizhao Xiong1,Aleksandar Matic1

Chalmers University of Technology1,Linköping University2,Uppsala University3,Institut Laue-Langevin4

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8:00 PM - CH01.04.03
Direct Insight into Electrochemical Processes in Alkali-Ion Cathodes from Operando Electron Spin Probes

Howie Nguyen1,Daniil Kitchaev1,Emily Foley1,Allyson Ee1,Yuefan Ji1,Raphaele Clement1

University of California, Santa Barbara1

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8:00 PM - CH01.04.04
Isothermal Microcalorimetry Characterization of Lithium Battery Storage Materials and Mechanisms

Wenzao Li1,Lisa Housel2,Calvin Quilty1,Mallory Vila1,Lei Wang2,Christopher Tang1,David Bock2,Kenneth Takeuchi1,2,Esther Takeuchi1,2,Amy Marschilok1,2

Stony Brook University1,Brookhaven National Laboratory2

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2021-12-01   Show All Abstracts

Symposium Organizers

Claire Villevieille, CEA
Kristina Edstrom, Uppsala University
Christian Masquelier, Université de Picardie Jules Verne
Y. Shirley Meng, University of California, San Diego
CH01.05: Multiscale Techniques
Session Chairs
Kent Griffith
Aleksandar Matic
Wednesday AM, December 1, 2021
Hynes, Level 3, Room 304

10:30 AM - *CH01.05.01
Insights into Battery Processes from the Perspective of the Electron Spin

Raphaele Clement1,Howie Nguyen1,Emily Foley1,Daniil Kitchaev1,Allyson Ee1,Yuefan Ji1

University of California, Santa Barbara1

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11:00 AM - CH01.05.02
Operando Surface Enhanced Raman Spectroelectrochemistry for Mechanistic Understanding of Energy Storage in Lithium/Sodium/Potassium Ion-Batteries Containing Few-Layered 2D Anodes

Mariusz Radtke1,Christian Hess1

Technical University of Darmstadt1

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11:15 AM - CH01.05.03
Elucidating the Role of Halides and Iron During Radiolysis Driven Oxidative Etching of Gold Nanocrystals Using Liquid Cell TEM and Pulse Radiolysis

Michelle Crook1,Christian Laube1,Ivan Moreno-Hernandez1,Axel Kahnt2,Stefan Zahn2,Justin Ondry1,Aijia Liu1,A. Paul Alivisatos1

University of California, Berkeley1,Leibniz Institute of Surface Engineering (IOM)2

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11:30 AM - CH01.05.04
Nanoscale Chemical and Structural Analysis During In Situ Scanning/Transmission Electron Microscopy in Liquids

Eric Stach1,3,Rui Serra-Maia1,Pawan Kumar1,Andrew Meng1,Alexandre Foucher1,Yijin Kang2,Deep Jariwala1,Khim Karki3

University of Pennsylvania1,Northwestern University2,Hummingbird Scientific3

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CH01.06: Spectroscopy Techniques I
Session Chairs
Raphaele Clement
Wednesday PM, December 1, 2021
Hynes, Level 3, Room 304

1:30 PM - *CH01.06.01
Exploring Complex Oxide Structural Motifs in Lithium-Ion Battery Anodes with Diffraction and Spectroscopy

Kent Griffith1,G. Snyder1,Kenneth Poeppelmeier1

Northwestern University1

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2:00 PM - CH01.06.02
Quantifying Electron-Beam Induced Electrochemistry Using In Situ KPFM

Evgheni Strelcov1,2,William McGehee1,Vladimir Oleshko1,Nikolai Zhitenev1,Jabez McClelland1,Andrei Kolmakov1

National Institute of Standards and Technology1,University of Maryland2

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2:15 PM - CH01.06.03
Illuminating Porous Electrodes via 4D In Situ Fluorescent Electrochemical Microscopy

Anton Graf1,Thomas Cochard1,Meisam Bahari1,Shmuel Rubinstein2,Michael Aziz1

Harvard University1,The Hebrew University of Jerusalem2

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2021-12-06   Show All Abstracts

Symposium Organizers

Claire Villevieille, CEA
Kristina Edstrom, Uppsala University
Christian Masquelier, Université de Picardie Jules Verne
Y. Shirley Meng, University of California, San Diego
CH01.11: Structural Characterization
Session Chairs
Claire Villevieille
Monday AM, December 6, 2021
CH01-Virtual

8:00 AM - *CH01.11.01
In Situ and Operando Neutron Powder Diffraction at the ILL on Li-Ion Batteries—How Can We Help You?

Emmanuelle Suard1

Institut Laue Langevin1

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8:30 AM - *CH01.11.02
CELLS-ALBA Synchrotron, a Versatile Facility Offering Wide Panel of In Situ and/or Operando Synchrotron Techniques Applied to Electrochemical Systems

Francois Fauth1

CELLS-ALBA synchrotron1

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9:00 AM - CH01.11.03
Resolving Structural Deterioration in Ni-Rich Layered Cathode Materials at Higher Operating Potentials in Operando

Anastasiia Mikheenkova1,Olof Gustafsson1,Casimir Misiewicz1,William Brant1,Matthew Lacey2,Maria Hahlin1,Erik Berg1

Uppsala University1,Scania CV AB2

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9:15 AM - CH01.11.04
LixMoO2 and NaxMoO2 Systems Studied by Operando Pair Distribution Function Analysis During Lithium or Sodium Electrochemical (De)Intercalation

Marie Guignard1,Matthew Suchomel1

Institute of Condensed Matter Chemistry of Bordeaux (ICMCB)1

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9:30 AM - *CH01.11.05
Operando Characterization of Silicon-Based Battery Anodes by Neutron and Synchrotron Techniques

Sandrine Lyonnard1

CEA-IRIG1

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CH01.12: Electrochemical Mechanisms
Session Chairs
Kristina Edstrom
Sandrine Lyonnard
Monday AM, December 6, 2021
CH01-Virtual

10:30 AM - *CH01.12.01
Towards Holistic Understanding of Electrochemical Energy Conversion and Storage Systems Using High Energy X-Rays

Jakub Drnec1

ESRF1

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11:00 AM - CH01.12.02
Advances in In Situ Liquid Phase TEM to Study Electrochemical Processes in Li-Ion Batteries and Beyond

Yevheniy Pivak1,Hongyu Sun1,Anne Beker1,Hugo Pérez Garza1

Denssolutions1

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11:15 AM - *CH01.12.03
Unriddling the Complex Battery Chemistry by Rationally Designed High-Performance Liquid Electrolytes

Isidora Cekic-Laskovic1

Helmholtz-Institute Muenster, IEK-12 Forschungszentrum Juelich1

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11:45 AM - CH01.12.04
Operando GCMS Gas Analysis for Monitoring Complex Electrolyte Decomposition Products in Lithium–Ion Batteries

Jürgen Kahr1,Christiane Groher1,Maria Antoniadou2,Erwin Rosenberg2,Marcus Jahn1

AIT1,Technische Universität Wien2

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12:00 PM - *CH01.12.05
Investigating Li Metal Anodes with Operando Neutron Depth Profiling and Solid-State NMR

Marnix Wagemaker1,Ming Liu1,Qidi Wang1,Chao Wang1,Tomas Verhallen1,Swapna Ganapathy1

Delft Univ of Technology1

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CH01.13: Interfacial Characterizations
Session Chairs
Jordi Cabana
Jakub Drnec
Monday PM, December 6, 2021
CH01-Virtual

1:00 PM - *CH01.13.01
Using X-Rays to Locate Chemical Phenomena in Battery Materials

Jordi Cabana1

University of Illinois at Chicago1

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1:30 PM - CH01.13.02
Imaging Phase Segregation in Nanostructured LixCoO2 Islands with Conductive Atomic Force Microscopy

Elliot Fuller1,David Ashby1,Celia Polop2,Enrique Vasco3,Joshua Sugar3,A. Talin1

Sandia National Laboratories1,Universidad Autónoma de Madrid2,Instituto de Ciencia de Materiales de Madrid3

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1:45 PM - CH01.13.03
In Situ X-Ray Multimodal Characterization for Insights into Synthesis/Processing of High-Ni Cathode Materials

Sizhan Liu1,Jianming Bai1,Feng Wang1

Brookhaven National Laboratory1

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2:00 PM - CH01.13.04
Advancing Nondestructive In Situ Characterizations of Buried Electrochemical Interfaces—Infrared Nanospectroscopy at Electrode/Liquid-Electrolyte and Electrode/Polymer-Electrolyte Interfaces

Jonathan Larson1,Xin He1,Hans Bechtel1,Robert Kostecki1

Lawrence Berkeley National Laboratory1

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2:15 PM - CH01.13.05
In Situ/Operando Soft X-Ray Absorption Spectroscopy Probing of the Electrode/Electrolyte Interfacial Dynamics Influenced by the Electrolyte Anions and Cations

Feipeng Yang1,Xuefei Feng1,Hui Li1,Scott McClary2,Ana Sanz-Matias1,Nathan Hahn2,David Prendergast1,Kevin Zavadil2,Jinghua Guo1

Lawrence Berkeley National Laboratory1,Sandia National Laboratories2

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2:30 PM - CH01.13.06
In Situ and Operando XPS Studies of the Si-Anode Solid-Electrolyte Interphase

Glenn Teeter1,Sarah Frisco1,Yeyoung Ha1,David Moore1,Andrew Colclasure1

National Renewable Energy Laboratory1

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2:45 PM - CH01.13.07
Operando Spectroscopic Ellipsometry—A Non-Destructive Optical Technique Offering Insights into Lithium Intercalation and Solid Electrolyte Interphase Formation

Juan Carlos Gonzalez-Rosillo1,Valerie Siller1,Marc Nuñez Eroles1,Michel Stchakovsky2,Alex Morata1,Albert Tarancon1,3

Catalonia Institute of Energy Research1,HORIBA Scientific2,ICREA3

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CH01.14: Dynamic Investigations
Session Chairs
Jordi Cabana
Y. Shirley Meng
Monday PM, December 6, 2021
CH01-Virtual

4:00 PM - *CH01.14.01
Operando Studies of Lithium-Ion Battery Electrodes Under Fast Charge Conditions

Daniel Abraham1

Argonne National Laboratory1

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4:30 PM - CH01.14.02
The Structure of the Electrical Double Layer on Graphene Suspended in Aqueous Salt Solutions—A Raman and Sum Frequency Vibrational Spectroscopy Study

Shanshan Yang1,Xiao Zhao1,Peidong Yang1,Miquel Salmeron1

Lawrence Berkeley National Laboratory1

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4:45 PM - CH01.14.03
In Situ Dynamic Measurements of Ti3C2 MXene Thin Films During Voltage Cycling at Variable Sweep Rates

Thomas Sobyra1,Tyler Mathis2,Yury Gogotsi2,Paul Fenter1

Argonne National Laboratory1,Drexel University2

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5:00 PM - *CH01.14.04
In Situ Magnetic Resonance Studies of Electrochemical Processes in Li-Ion Cells Using Novel Probes

Gillian Goward1,Kevin Sanders1,Amanda Ciezki1,Zoya Sadighi1,Annica Freytag1,Andres Ramírez Aguilera2,Bruce Balcom2

McMaster University1,University of New Brunswick2

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5:30 PM - CH01.14.05
Structural Dynamics of Metallic Nanocatalysts for Fuel Cells by In Situ Total X-Ray Scattering

Valeri Petkov1

Central Michigan University1

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5:45 PM - CH01.14.06
In Operando Study of Electrochemical Strain and Charge Storage in Nanosheet Oxide Electrodes

Scott Misture1,Madeleine Flint1,Peter Metz1,Peng Gao1,Robert Koch1

Alfred University1

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CH01.15: Morphological and Structural Characterization
Session Chairs
Daniel Abraham
Gillian Goward
Monday PM, December 6, 2021
CH01-Virtual

6:30 PM - *CH01.15.01
Advanced Neutron Characterisation of Rechargeable Batteries

Vanessa Peterson1,2

ANSTO1,University of Wollongong2

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7:00 PM - CH01.15.02
In Situ TEM Corrosion Study and Anti-Corrosion Control of Pd@Pt Core-Shell Electrocatalysts

Fenglei Shi1

Shanghai Jiao Tong University1

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7:15 PM - CH01.15.03
Operando Visualization of Mass Transport Behavior in Electrolytes During Electrochemical Device Operation by Phase-Contrast X-Ray Imaging

Daiko Takamatsu1,Akio Yoneyama1,Jun Hayakawa1

Hitachi, Ltd.1

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7:30 PM - *CH01.15.04
Structural-Electrochemical Studies of Sodium-Ion Battery Positive Electrodes

Neeraj Sharma1

UNSW1

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8:00 PM - *CH01.15.05
Operando Analysis of Lithium-Ion Battery Electrodes and Cells Featuring Neutron Diffraction

Hajime Arai1,Tetsuya Omiya1,Atsunori Ikezawa1

Tokyo Institute of Technology1

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2021-12-07   Show All Abstracts

Symposium Organizers

Claire Villevieille, CEA
Kristina Edstrom, Uppsala University
Christian Masquelier, Université de Picardie Jules Verne
Y. Shirley Meng, University of California, San Diego
CH01.16: Imaging and Structural Characterization
Session Chairs
Francois Fauth
Emmanuelle Suard
Tuesday AM, December 7, 2021
CH01-Virtual

10:30 AM - *CH01.16.01
Understanding the Interplay of Electrode Microstructure, Crystallography and Performance Using Advanced X-Ray and Correlative Imaging Methods

Paul Shearing1,2

University College London1,The Faraday Institution2

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11:00 AM - CH01.16.02
Revealing a Dissolution and Reprecipitation Process of Copper Catalysts During CO2 Reduction Reaction

Jan Vavra1,Tzu-Hsien Shen1,Dragos Stoian1,Vasiliki Tileli1,Raffaella Buonsanti1

EPFL1

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11:15 AM - *CH01.16.03
Atoms in Motion—Operando M-Ion Battery Monitoring Using X-Ray Techniques

Montserrat Casas-Cabanas1,Damien Saurel1,Marine Reynaud1,María Jáuregui1,Montserrat Galcerán1

CIC Energigune1

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11:45 AM - *CH01.16.04
Visualizing Electrochemical Reactions at the Nano- and the Atomic Scale by In Situ TEM

Huolin Xin1,Chunyang Wang1,Lili Han1,Peichao Zou1

University of California, Irvine1

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12:15 PM - CH01.16.05
In Situ NMR Guided Electrochemical Regeneration of Anthraquinone Flow Batteries

Yan Jing1,Evan Wenbo Zhao2,Marc-antonio Goulet1,Meisam Bahari1,Eric Fell1,Shijian Jin1,Erlendur Jónsson2,Ali Davoodi1,Min Wu1,Clare Grey2,Roy Gordon1,Michael Aziz1

Harvard University1,University of Cambridge2

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CH01.17: Microscopy and Imaging Techniques & Poster Session II
Session Chairs
Tuesday PM, December 7, 2021
CH01-Virtual

1:00 PM - *CH01.17.01
Fast X-Ray Operando Measurements “at Home”

Jean-Noel Chotard1,Vincent Seznec1,Arina Nadeina1,Tristan Lombard1,Christian Masquelier1

Lab de Reactivite Chimie-Solides1

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1:30 PM - CH01.17.02
Operando X-Ray Nano-CT Coupling with XANES for Monitoring the (De)Lithiation Dynamics Inside NMC Secondary Particle

Arnaud Demortiere1,Tuan-Tu Nguyen1,Zeliang Su1,Vincent De Andrade2,Charles Delacourt1

CNRS RS2E/LRCS1,Argonne National Laboratory2

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1:45 PM - CH01.17.03
Late News: Advances in Direct Detectors for In Situ Electron Microscopy

Barnaby Levin1

Direct Electron LP1

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2:00 PM - CH01.17.04
Late News: Anisotropy of Lithium Metal Stripping Explored with Operando 3D Microscopy

Adrian Sanchez1,Eric Kazyak1,Yuxin Chen1,Jose Lasso1,Neil Dasgupta1

University of Michigan1

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2:15 PM - CH01.17.05
Late News: In Situ Transmission Electron Microscopy of High-Temperature Corrosion by Chloride Salts

Prachi Pragnya1,Daniel Gall1,Robert Hull1

Rensselaer Polytechnic Institute1

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2:30 PM - CH01.17.06
Far-Infrared Spectroelectrochemistry for Investigating Organometallic Structures

Lucyano Macedo1,Frank Crespilho1

University of São Paulo1

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2:35 PM - CH01.17.07
Reaction Rate Constant Parameterization Methods for Simplified Electrochemical Lithium-Ion Models

Alain Goussian1,Sylvain Franger1,Loïc Assaud1,Issam Baghdadi2

Université Paris-Saclay1,Stellantis2

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2:40 PM - CH01.17.08
Chloride Assisted Corrosion of Copper and Protection by Benzotriazole

Shanshan Yang1,Xiao Zhao1,Miquel Salmeron1

Lawrence Berkeley National Laboratory1

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2:45 PM - CH01.17.09
Solid-Liquid Interactions of Oxygen Evolving Oxide Catalysts Probed in Real-Time

Tzu-Hsien Shen1,Liam Spillane2,Jiayu Peng3,Yang Shao-Horn3,Vasiliki Tileli1

Ecole Polytechnique Federale de Lausanne1,Gatan2,Massachusetts Institute of Technology3

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2021-12-08   Show All Abstracts

Symposium Organizers

Claire Villevieille, CEA
Kristina Edstrom, Uppsala University
Christian Masquelier, Université de Picardie Jules Verne
Y. Shirley Meng, University of California, San Diego
CH01.18: Imaging and Surface Characterization
Session Chairs
Jean-Noel Chotard
Arnaud Demortiere
Wednesday AM, December 8, 2021
CH01-Virtual

8:00 AM - *CH01.18.01
Mapping Lithium with Operando Synchrotron X-Ray and Neutron Imaging Techniques

Ingo Manke1,Markus Osenberg1,Nikolay Kardjilov1,Robert Bradbury1,Wolfgang Zeier2,Ohno Saneyuki3,Alessandro Tengattini4,André Hilger1,Joachim Binder5,Kang Dong1,Fu Sun6

Helmhotz-Zentrum Berlin1,University Münster2,Kyushu University3,Universite Grenoble4,Karlsruhe Institute of Technology5,Chinese Academy of Sciences6

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8:30 AM - CH01.18.02
Operando Atomic Force Microscope-Scanning Electrochemical Microscopy (AFM-SECM) of pH Gradients at Gas Diffusion Electrodes

Nathan Nesbitt1,2,Thomas Burdyny2,Divya Bohra2,Recep Kas3,2,Wilson Smith1,3,2

National Renewable Energy Laboratory1,TU Delft2,University of Colorado Boulder3

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8:45 AM - *CH01.18.03
Operando Kerr Gated Raman Spectroscopy to Investigate Ageing Processes on Lithium-Ion Electrode Interfaces

Laurence Hardwick1,Alex Neale1,David Costa-Milan1,Laura Cabo-Fernandez1,Filipe Braga1,Igor Sazanovich2

University of Liverpool1,Central Laser Facility2

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9:15 AM - CH01.18.04
Improved Operando Raman Cell Configuration for Commercially-Sourced Li-Ion and Na-Ion Battery Electrodes

Andy Wain1,Tim Rosser1,Edmund Dickinson1,Rinaldo Raccichini1,Katherine Hunter2,Andrew Searle2,Christopher Kavanagh2,Peter Curran2,Gareth Hinds1,Juyeon Park1

National Physical Laboratory1,Deregallera Ltd2

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9:30 AM - CH01.18.06
Revisiting the Ethylene Carbonate–Propylene Carbonate Mystery with Operando Characterization

Tim Melin1,Erik Berg1

Uppsala University1

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9:45 AM - CH01.19.05
Elucidating Performance-Limiting Side-Reactions in Large-Format Li-Ion Cells with Operando Electrochemical Mass Spectrometry

Casimir Misiewicz1

Uppsala University1

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CH01.19: Bulk and Interfacial Investigation
Session Chairs
Ingo Manke
Wednesday AM, December 8, 2021
CH01-Virtual

10:30 AM - *CH01.19.01
Effective Transport in Li-S Solid–State Batteries

Wolfgang Zeier1

University of Muenster1

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11:00 AM - CH01.19.02
Operando Surface Enhanced Raman Spectroscopy of the Stepwise Formation of Solid Electrolyte Interphases in Li-Ion Batteries

Neeha Gogoi1,Erik Berg1

Uppsala University1

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11:15 AM - CH01.19.03
The Effects of Residual Water in Li-Ion Battery Model Systems Studied with Online Gas Analysis

Robin Lundström1,Erik Berg1

Uppsala University1

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11:30 AM - *CH01.19.04
Using In Situ X-Ray Spectroscopy to Study Metal-Sulfur Batteries

Lorenzo Stievano1,2

Univ. Montpellier1,RS2E2

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12:00 PM - CH01.19.06
Operando X-Ray Scattering with Stochastic Modelling to Quantify the Nanoscale Phase Evolution in Post-Lithium-Ion Batteries

Christian Prehal1,2,Heinz Amenitsch2,Stefan Freunberger3,2,Vanessa Wood1

ETH Zurich1,Graz University of Technology2,IST Austria (Institute of Science and Technology Austria)3

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CH01.20: Probing Interfaces
Session Chairs
Wednesday PM, December 8, 2021
CH01-Virtual

1:00 PM - *CH01.20.01
Probing Interface Stability and Charge Distribution in Solid-State Batteries via STEM

Miaofang Chi1

Oak Ridge National Laboratory1

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1:30 PM - CH01.20.02
Using High Energy Synchrotron Diffraction to Probe Spatial and Temporal Heterogeneities in Lithium-Ion Batteries—Graphite Anode, NMC Cathode and Lithium Plating

Harry Charalambous1,Kamila Wiaderek1,Yang Ren1

Argonne National Laboratory1

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1:45 PM - CH01.20.04
Modelling X-Ray Absorption Spectra for Dynamic Interfaces in Multivalent Electrolytes

Ana Sanz-Matias1,David Prendergast1

Lawrence Berkeley National Laboratory1

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2:00 PM - CH01.04.01
Nucleation and Growth of Transition Metal Alloy Nanoparticles from Transition Metal Hydroxide Complexes Observed in Graphene Liquid Cells

Azadeh Amiri1,Abhijit Phakatkar1,Reza Shahbazian-Yassar1

University of Illinois Chicago1

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2:05 PM - CH01.04.05
In Situ Transmission Electron Microscopy Studies of Multi-Elemental Nanoparticles Synthesis in Liquid Flow Cells

Azadeh Amiri1,Abhijit Phakatkar1,Reza Shahbazian-Yassar1

University of Illinois Chicago1

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2:10 PM - CH01.01.03
Operando XRD and Lattice Models as Tools to Determine Phase Diagrams—The Case of LiNiO2

Matteo Bianchini1,2,Markus Mock1,Francois Fauth3,Karsten Albe4,Sabrina Sicolo1

BASF SE1,Karlsruhe Institute of Technology2,ALBA Synchrotron3,Technische Universität Darmstadt4

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2:25 PM - CH01.03.03
Structural Evolution of All-Solid-State Li-Ion Battery Using Operando TEM and X-Ray Micro-CT

Sorina Cretu1,2,3,Martial Duchamp2,Arnaud Demortiere1,3,4

Laboratoire de Réactivité et de Chimie des Solides1,Nanyang Technological University2,RS2E-French Research Network on Electrochemical Energy Storage3,ALISTORE- European Research Institute4

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