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2014 MRS Spring Meeting Logo2014 MRS Spring Meeting & Exhibit

April 21-25, 2014 | San Francisco
Meeting Chairs: Jose A. Garrido, Sergei V. Kalinin, Edson R. Leite, David Parrillo, Molly Stevens


Symposium CCC : In-situ Characterization of Material Synthesis and Properties at the Nanoscale with TEM

2014-04-22   Show All Abstracts

Symposium Organizers

Renu Sharma, National Institute of Standards and Technology
Miaofang Chi, Oak Ridge National Laboratory
Jonathan Winterstein, FEI Company
Zhiwei Shan, Xi'an Jiaotong University

Symposium Support

FEI Company
Gatan, Inc.
Hysitron, Inc.
Protochips, Inc.
CCC2: In situ TEM of Phase Transformations
Session Chairs
Miaofang Chi
Judith Yang
Tuesday PM, April 22, 2014
Moscone West, Level 3, Room 3011

2:30 AM - *CCC2.01
Inducing Phase Transformations In-Situ with Electrical Current and Electron Beam

Jae Hyuck Jang 1 Donovan N Leonard 1 Young-Min Kim 2 Qian He 1 Amit Kumar 1 Stephen J Pennycook 1 Sergei V Kalinin 1 Albina Y Borisevich 1

1Oak Ridge National Laboratory Oak Ridge USA2Korea Basic Science institute Daejeon Republic of Korea

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3:00 AM - CCC2.02
In-Situ Nanocalorimetry with Time-Resolved Electron Microscopy for the Study of Rapid Phase Transformations

Michael D. Grapes 1 3 Thomas LaGrange 2 Bryan W. Reed 2 Geoffrey H. Campbell 2 David A. LaVan 3 Timothy P. Weihs 1

1Johns Hopkins University Baltimore USA2Lawrence Livermore National Laboratory Livermore USA3National Institute of Standards and Technology Gaithersburg USA

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3:15 AM - CCC2.03
Mechanisms of Anatase-to-Rutile Phase Transformation and Branched TiO2 Nanowire Growth

Dongsheng Li 1 Jim De Yoreo 1

1PNNL Richland USA

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3:30 AM - CCC2.04
In-Situ TEM Studies of Structure-Property Evolution in GeTe Nanowire Phase-Change Memory During Crystal-to-Amorphous Transformation

Pavan Nukala 1 Rahul Agarwal 1 Xiaofeng Qian 2 Moon Hyung Jang 1 Sajal Dhara 1 Karthik Kumar 1 Charlie Johnson 1 3 Ju Li 2 Ritesh Agarwal 1

1University of Pennsylvania Philadelphia USA2Massachusetts Institute of Technology Cambridge USA3University of Pennsylvania Philadelphia USA

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3:45 AM - CCC2.05
High-Resolution TEM of CdSe Nanorod Sublimation

Daniel Hellebusch 1 2 3 Karthish Manthiram 1 2 3 A. Paul Alivisatos 2 3

1University of California, Berkeley Berkeley USA2University of California, Berkeley Berkeley USA3Lawrence Berkeley National Laboratory Berkeley USA

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4:00 AM - CCC2
Break

4:30 AM - *CCC2.06
Structural Dynamics of Supported Metal Nano-Clusters Using Electron Microscopy, In-Situ X-Ray Spectroscopy, and Theoretical Simulations

Judith C Yang 1

1University of Pittsburgh Pittsburgh USA

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5:00 AM - CCC2.07
Electron Correlation Microscopy: A New Technique for Measuring Atomic Rearrangements at the Nanoscale

Li He 1 Chia-Lin Li 2 Jinn Chu 2 Peter Liaw 3 Paul Voyles 1

1University of Wisconsin, Madison Madison USA2National Taiwan University of Science and Technology Taipei Taiwan3University of Tennessee Knoxville USA

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5:15 AM - CCC2.08
Understanding In-Situ STEM Images Through Atomistic Simulations of Model Systems

David Alan Welch 1 Layla Mehdi 2 Taylor Woehl 1 Chiwoo Park 4 James E. Evans 3 Roland Faller 1 Nigel D. Browning 2

1University of California-Davis Davis USA2Pacific Northwest National Laboratory Richland USA3Pacific Northwest National Laboratory Richland USA4Florida State University Tallahassee USA

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5:30 AM - CCC2.09
Atomic Scale Dynamics of a Solid State Chemical Reaction Uncovered by Z-Contrast Electron Microscopy

Timothy J Pennycook 1 2 Lewys Jones 1 Henrik Petterson 3 Valeria Nicolosi 3 Peter Nellist 1 2

1University of Oxford Oxford United Kingdom2SuperSTEM Daresbury United Kingdom3Trinity College Dublin Dublin United Kingdom

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CCC1: Nanoscale Mechanical Behavior Studied with TEM
Session Chairs
Zhiwei Shan
Lian-Mao Peng
Tuesday AM, April 22, 2014
Moscone West, Level 3, Room 3011

9:00 AM - *CCC1.01
In-Situ Electron Microscopy and Micro-Laue Study of Plasticity in Miniaturized Cu Bicrystals

Peter J. Imrich 1 Christoph Kirchlechner 2 Christian Motz 3 Gerhard Dehm 2

1Erich Schmid Institute of Materials Science Leoben Austria2MPI-Eisenforschung Duesseldorf Germany3Department of Materials Science Saarbramp;#252;cken Germany

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CCC3: Poster Session: In situ TEM
Session Chairs
Tuesday PM, April 22, 2014
Marriott Marquis, Yerba Buena Level, Salons 8-9

9:00 AM - CCC3.02
In-Situ Observation of Compressive Deformation in Metallic Glass Nanoparticles

Jin Woo Kim 1 Hye Jung Chang 2 Eun Soo Park 1

1Seoul National University Seoul Republic of Korea2Korea Institute of Science and Technology Seoul Republic of Korea

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9:00 AM - CCC3.04
In-Situ TEM High Temperature Deformation Behavior in Nanoscale Pt Thin Films

Sandeep Kumar 1 Aman Haque 2

1UC, Riverside Riverside USA2Penn State University University park USA

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9:00 AM - CCC3.07
Microstructure and the Strengthening Mechanism of Nano-Twinned Cu with Controlled Orientation Using Cs-Corrected TEM

Yi-Chia Chou 1 Hsuan Lin 1 Chia-Ling Lu 2 Chih Chen 2 King-Ning Tu 3

1National Chiao Tung University Hsinchu Taiwan2National Chiao Tung University Hsinchu Taiwan3UCLA Los Angeles USA

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9:00 AM - CCC3.08
In-Situ UHVEM Study of {113}-Defect Generation in Si Nanowires

Jan Vanhellemont 1 2 Satoshi Anada 1 Takeshi Nagase 1 Hidehiro Yasuda 1 Hugo Bender 3 Rita Rooyackers 3 Anne Vandooren 3

1Osaka University Osaka Japan2Ghent University Ghent Belgium3IMEC Leuven Belgium

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9:00 AM - CCC3.10
Quantitative Atomistic Observation of Small Au Nanoparticle Coalescence and Migration by Aberration-Corrected Scanning Transmission Electron Microscopy

Yan Xin 1

1Florida State University Tallahassee USA

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9:00 AM - CCC3.11
Dynamics of Pd Nanocubes Observed Using In-Situ Liquid-Cell Transmission Electron Microscopy: Chemical Etching and Beam Induced Rotation

Yingying Jiang 1 Guomin Zhu 1 Hui Zhang 1 Daan Hein Alsem 2 See Wee Chee 2 Chuanhong Jin 1

1Zhejiang University Hangzhou China2Hummingbird Scientific Lacey USA

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9:00 AM - CCC3.12
In-Situ (S)TEM Fabrication of Graphene Nanoribbon-Nanopore Devices for DNA Sequencing

Julio Alejandro Rodriguez-Manzo 1 Matthew Puster 1 2 Adrian Balan 1 Marija Drndic 1

1University of Pennsylvania Philadelphia USA2University of Pennsylvania Philadelphia USA

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9:00 AM - CCC3.13
Field Emission Characteristics of Vertical Few-Layer Graphene Using In-Situ TEM

Yu Zhang 1 Shuai Tang 1 Shaozhi Deng 1 Jun Chen 1 Ningsheng Xu 1

1Sun Yat-sen University Guangzhou China

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9:00 AM - CCC3.14
In-Situ Observation of Electroless Copper Deposition Process in K-kit by Transmission Electron Microscopy

Shih-En Lai 1 Tri-Rung Yew 1

1National Tsing Hua University Hsinchu Taiwan

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9:00 AM - CCC3.15
Atomic Resolution Transmission Electron Microscopy of Defect Dynamics in Hexagonal Boron Nitride and Graphene

Ashley Gibb 1 2 4 Nasim Alem 5 4 Chengyu Song 4 Jim Ciston 4 Alex Zettl 2 3

1UC Berkeley Berkeley USA2UC Berkeley Berkeley USA3Lawrence Berkeley National Lab Berkeley USA4Lawrence Berkeley National Lab Berkeley USA5The Pennsylvania State University University Park USA

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9:00 AM - CCC3.16
In-Situ TEM Study of Metal Nanoparticles Sintering

Yuzi Liu 1 Yugang Sun 1

1Argonne National Laboratory Argonne USA

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9:00 AM - CCC3.17
In-Situ SEM Study of Lithium Intercalation in V2O5 Nanowires

Evgheni Strelcov 1 2 Joshua Cothren 1 Donovan Leonard 3 Sergei V. Kalinin 2 Albina Y. Borisevich 3 Andrei Kolmakov 1 4

1Southern Illinois University at Carbondale Carbondale USA2Oak Ridge National Lab Oak Ridge USA3Oak Ridge National Lab Oak Ridge USA4National Institute of Standards and Technology Gaithesburg USA

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9:00 AM - CCC3.18
Manganese Silicide/Silicon Nanowire Heterostructures: In-Situ TEM Observation of Growth Mechanism and Their Physical Properties

Yu-Shun Hsieh 1 Chun-Wei Huang 1 Chung-Hua Chiu 1 Kuo-Chang Lu 1 Wen-Wei Wu 1

1National Chiao Tung University Hsinchu Taiwan

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CCC1: Nanoscale Mechanical Behavior Studied with TEM
Session Chairs
Zhiwei Shan
Lian-Mao Peng
Tuesday AM, April 22, 2014
Moscone West, Level 3, Room 3011

9:30 AM - *CCC1.02
In-Situ Microscopy Study on Transition of Plasticity Mechanism of Nanomaterials

Ze Zhang 1 X. D. Han 2

1Zhejiang University Hangzhou China2Beijing University Beijing China

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10:00 AM - CCC1.03
In-Situ TEM Observation of Twin Boundary Migration in Copper Nanotwinned Pillars

Zhangjie Wang 1 Qingjie Li 2 Mingyu Xu 1 Yang Lu 3 Ming Dao 4 Ju Li 4 5 1 Jun Sun 1 Evan Ma 2 1 Zhiwei Shan 1

1Xiamp;#8217;an Jiaotong University Xi'an China2Johns Hopkins University Baltimore USA3City University of Hong Kong Hong Kong Hong Kong4Massachusetts Institute of Technology Boston USA5Massachusetts Institute of Technology Boston USA

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10:15 AM - CCC1.04
In-Situ Characterization of Dislocation-Grain Boundary Interaction by TEM Nanoindentation

Shun Kondo 1 Tasuku Mitsuma 1 Eita Tochigi 2 Naoya Shibata 2 Yuichi Ikuhara 2

1The University of Tokyo Yayoi, Bunkyo-ku Japan2The University of Tokyo Yayoi, Bunkyo-ku Japan

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10:30 AM - CCC1.05
Characterization of Nano-Mechanical Behavior Associated with an Evolution of Dislocation Structure During Micro-Compression of BCC Iron

Takahito Ohmura 1 Ling Zhang 1 Nobuaki Sekido 1

1National Institute for Materials Science Tsukuba Japan

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10:45 AM - CCC1.06
New Insights into Adhesion and Wear from In-Situ TEM Studies

Robert W. Carpick 1 Tevis D.B. Jacobs 1 Joel A. Lefever 1 Jingjing Liu 2 David S. Grierson 3 Kathleen E. Ryan 4 Pamela L Keating 4 Judith A. Harrison 4

1University of Pennsylvania Philadelphia USA2Applied Materials Santa Clara USA3systeMECH, LLC Madison USA4United States Naval Academy Annapolis USA

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11:00 AM - CCC1
Break

11:30 AM - *CCC1.07
In-Situ TEM Probing of Mechanical and Electromechanical Properties

Andrew M Minor 1

1UC Berkeley amp; LBL Berkeley USA

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12:00 PM - CCC1.08
Hollow Spherical Structures for High Performance Energy Absorption

Shimin Mao 1 Baoxing Xu 1 Hangxun Xu 2 Jim Mabon 3 Waclaw Swiech 3 Shen Dillon 1

1University of Illinois Urbana Champaign Urbana USA2University of Science and Technology of China, CAS Key Laboratory of Soft Matter Chemistry Hefei China3University of Illinois Urbana Champaign Urbana USA

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12:15 PM - CCC1.09
In-Situ Nanoindentation of Dealloyed Nanoporous Silicon

Xu Jiang 1 John Balk 1

1University of Kentucky Lexington USA

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12:30 PM - *CCC1.10
Characterizing Individual Nanostructures: Structure, Electrical, Mechanical and Optical Properties

Lian-Mao Peng 1

1Peking University Beijing China

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2014-04-23   Show All Abstracts

Symposium Organizers

Renu Sharma, National Institute of Standards and Technology
Miaofang Chi, Oak Ridge National Laboratory
Jonathan Winterstein, FEI Company
Zhiwei Shan, Xi'an Jiaotong University

Symposium Support

FEI Company
Gatan, Inc.
Hysitron, Inc.
Protochips, Inc.
CCC5: TEM of Materials in a Liquid Environment
Session Chairs
Jonathan Winterstein
Wednesday PM, April 23, 2014
Moscone West, Level 3, Room 3011

2:30 AM - *CCC5.01
Scanning Transmission Electron Microscopy of Whole Eukaryotic Cells in Liquid and In-Situ Studies of Nanomaterials

Niels de Jonge 1 Diana B Peckys 1 Tobias Schuh 1

1INM-Leibniz Institute for New Materials Saarbruecken Germany

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3:00 AM - CCC5.02
High Precision In-Situ Study of Reactions in Thin Window Liquid Cells

Canhui Wang 1 Qiao Qiao 1 Tolou Shokuhfar 2 1 Robert Klie 1

1University of Illinois at Chicago Chicago USA2Michigan Technological University Houghton USA

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3:15 AM - CCC5.03
Quantitative (S)TEM/DTEM Observations of Nanomaterials Dynamics in Liquids

Patricia Abellan 1 Taylor J. Woehl 2 Lucas R. Parent 2 Meng Gu 3 Beata L. Mehdi 1 Ilke Arslan 4 Chongmin Wang 3 Chiwoo Park 5 W. Andreas Schroeder 6 James E. Evans 3 Nigel D Browning 1

1Pacific Northwest National Laboratory Richland USA2University of California-Davis Davis USA3Pacific Northwest National Laboratory Richland USA4Pacific Northwest National Laboratory Richland USA5Florida State University Tallahassee USA6University of Illinois at Chicago Chicago USA

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3:30 AM - CCC5
Break

4:00 AM - *CCC5.04
Radiolysis Induced by the Electron Beam and Its Implications

Nicholas M. Schneider 2 Michael M. Norton 2 Brian J. Mendel 2 Joseph M. Grogan 2 3 Frances M. Ross 1 Haim H. Bau 2

1IBM T. J. Watson Research Center Yorktown Heights USA2University of Pennsylvania Philadelphia USA3Hummingbird Scientific Lacey USA

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4:30 AM - CCC5.05
Correlating Nanoparticle Nucleation and Growth Mechanisms with Cyclic Voltammetry and In-Situ ec-S/TEM Characterization

Raymond Unocic 1 Robert Sacci 2 Gilbert Brown 3 Nancy Dudney 2 Karren More 1

1Oak Ridge National Laboratory Oak Ridge USA2Oak Ridge National Laboratory Oak Ridge USA3Oak Ridge National Laboratory Oak Ridge USA

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4:45 AM - CCC5.06
In-Situ Observation of Nucleation and Growth on Nanocrystals of Controlled Shapes Using Liquid Cell

Jianbo Wu 1 2 Wenpei Gao 2 3 See Wee Chee 4 Hong Yang 1 Jian-Min Zuo 2 3

1University of Illinois Urbana USA2University of Illinois Urbana USA3University of Illinois Urbana USA4Hummingbird Scientific Lacey USA

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5:00 AM - CCC5.07
Application of In-Situ Liquid Electrochemical TEM Cell to Study Growth Mechanism of Li2O2 Nanoparticles in Li-O2 Battery

B. Layla Mehdi 1 Eduard N. Nasybulin 2 Meng Gu 3 Patricia Abellan 1 Lucas R Parent 1 James E Evans 3 Chongmin Wang 3 Wu Xu 2 Jiguang G Zhang 2 Nigel D Browining 1

1Pacific Northwest National Laboratory Richland USA2Pacific Northwest National Laboratory Richland USA3Pacific Northwest National Laboratory Richland USA

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5:15 AM - CCC5.08
Correlative Light/Electron Microscopy by Using Graphene Liquid Cells

Jungwon Park 1 Ji Tae Park 1 Jun Byun 1 David A. Weitz 1

1Harvard University Cambridge USA

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5:30 AM - CCC5.09
In-Situ Electron Holography Study of a Magnetic Read/Write Recording Head in Operation

Etienne Snoeck 1 Christophe Gatel 1 Aurelien Masseboeuf 1 Robin Cours 1 Joshua F. Einsle 2 Robert M. Bowman 2 Mark Gubbins 3 Muhammad Bashir 3

1CNRS Toulouse France2Queens University Belfast United Kingdom3Seagate Technology Londonderry United Kingdom

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5:45 AM - CCC5.10
Elementary Charge Measurement during Field Emission on a Carbon Cone Nanotip Studied by In-Situ Electron Holography

Christophe Gatel 1 2 Ludvig de Knoop 1 2 Florent Houdellier 1 2 Auramp;#233;lien Masseboeuf 1 2 Marc Monthioux 1 2 Etienne Snoeck 1 2 Martin James Hytch 1 2

1CEMES-CNRS Toulouse France2University of Toulouse Toulouse France

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CCC4: Environmental Transmission Electron Microscopy
Session Chairs
Renu Sharma
Peter Crozier
Wednesday AM, April 23, 2014
Moscone West, Level 3, Room 3011

9:30 AM - *CCC4.01
Dynamical Environmental TEM: Time Resolution for In-Situ Electron Microscopy

Jian Min Zuo 1 2 Yang Hu 1 2 Wenpei Gao 1 2 Jianbo Wu 1 2

1University of Illinois Champaign-Urbana USA2University of Illinois champaign-Urbana USA

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10:00 AM - CCC4.02
In-Situ TEM Observation of Branching in CdS Nanobelts

Rahul Agarwal 1 Dmitri Zakharov 2 Eric A Stach 2 Ritesh Agarwal 1

1University of Pennsylvania PHILADELPHIA USA2Brookhaven National Laboratory Upton USA

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10:15 AM - CCC4.03
In-Situ Single Nanoparticle Studies of Hydrogen Loading in Palladium

Tarun Narayan 1 Andrea Baldi 1 2 Ai Leen Koh 3 Jennifer Dionne 1

1Stanford University Stanford USA2FOM Institute AMOLF Amsterdam Netherlands3Stanford University Stanford USA

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10:45 AM - CCC4
Break

11:15 AM - *CCC4.05
Comparative Evolution of Nanomaterials in Gas Atmospheres During Thermal, Electron and Light Stimuli

Peter A Crozier 1

1Ariaona State Unversity Tempe USA

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11:45 AM - CCC4.06
Correlative Electron Microscopy and Photon Science Characterization of Working Catalysts

Eric A. Stach 1 Yuanyuan Li 2 Dmitri Zakharov 1 Ralph Nuzzo 3 Anatoly Frenkel 2

1Brookhaven National Lab Upton USA2Yeshiva University New York USA3University of Illinois - Urbana Champaign Urbana USA

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12:00 PM - CCC4.07
Optical Spectroscopy Integrated with Environmental Scanning Transmission Electron Microscopy: A Comprehensive In-Situ Characterization

Matthieu Claude Picher 1 2 Steve Blankenship 1 Stefano Mazzucco 1 Renu Sharma 1

1Institute of Standards and Technology Gaithersburg USA2University of Maryland College Park USA

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12:15 PM - CCC4.08
Photochemical Structural Evolution of Metal/TiO2 Photocatalysts During Light Irradiation in an Environmental Transmission Electron Microscope

Liuxian Zhang 1 Peter Crozier 1

1Arizona State University Tempe USA

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2014-04-24   Show All Abstracts

Symposium Organizers

Renu Sharma, National Institute of Standards and Technology
Miaofang Chi, Oak Ridge National Laboratory
Jonathan Winterstein, FEI Company
Zhiwei Shan, Xi'an Jiaotong University

Symposium Support

FEI Company
Gatan, Inc.
Hysitron, Inc.
Protochips, Inc.
CCC6: Nanoscale Electrochemistry with TEM
Session Chairs
Miaofang Chi
Albina Borisevich
Thursday AM, April 24, 2014
Moscone West, Level 3, Room 3011

9:30 AM - *CCC6.01
In-Situ Analytical Electron Microscopy for Probing Electrochemistry at Nano-Scale

Shirley Meng 1 Dhamodaran Santhanagopalan 1 Ziying Wang 1 Nancy Dudney 2 Feng Wang 3

1University of California San Diego La Jolla USA2Oak Ridge National Lab Oak Ridge USA3Brookhaven National Lab Brookhaven USA

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10:00 AM - CCC6.02
In Operando (S)TEM Observations of Li-ion Battery Processes During Electrochemical Lithiation/Delithiation of Si Nanowire Electrodes

Lucas R. Parent 1 Meng Gu 2 Patricia Abellan 2 Layla Mehdi 2 Raymond R. Unocic 3 Yi Cui 4 James E. Evans 2 Chongmin Wang 2 Nigel D. Browning 1 2 Ilke Arslan 2

1University of California, Davis Davis USA2Pacific Northwest National Laboratory Richland USA3Oak Ridge National Laboratory Oak Ridge USA4Stanford University Stanford USA

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10:15 AM - CCC6.03
Atomic-Scale Real-Time Observation of Crystal Shrinkage in LiFePO4 at High Temperature

Sung-Yoon Chung 1 2

1KAIST Daejeon Republic of Korea2Nalphates LLC Wilmington USA

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10:30 AM - CCC6.04
In-Situ I-V Measurements at Unipolar Resistive Switching Pt/SrTiO3/Pt System

Deok-Hwang Kwon 1 Shin Buhm Lee 2 3 Chan Soon Kang 1 Seung-Yong Lee 1 Hye-Lim Cho 1 Kyu Hwan Oh 1 Tae Won Noh 2 3 Miyoung Kim 1

1Seoul National University Seoul Republic of Korea2Seoul National University Seoul Republic of Korea3Seoul National University Seoul Republic of Korea

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10:45 AM - CCC6
Break

11:15 AM - *CCC6.05
In-Situ TEM-EELS Studies of Electronic and Ionic Transport in Electrodes for Li-Ion Batteries

Feng Wang 1 Peng Gao 1 Sung-Wook Kim 1 Lijun Wu 1 Dong Su 1 Jason Graetz 1 Yimei Zhu 1

1Brookhaven National Laboratory Upton USA

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11:45 AM - CCC6.06
Real-Time Observation of Vacancy Dynamics and Phase Transformation in Epitaxial LaCoO3-x Thin Films

Jae Hyuck Jang 1 Young-Min Kim 2 Qian He 1 Liang Qiao 3 Michael D. Biegalski 3 Andrew R. Lupini 1 Stephen J. Pennycook 1 Sergei V. Kalinin 3 Albina Y. Borisevich 1

1Oak Ridge National Laboratory Oak Ridge USA2Korea Basic Science institute Daejeon Republic of Korea3Oak Ridge National Laboratory Oak Ridge USA

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12:00 PM - CCC6.07
Understanding Mechanisms of Electric Field Assisted Sintering Using a Variety of In situ TEM Experiments

Hasti Majidi 1 Jorgen F Rufner 1 Troy B Holland 2 Klaus van Benthem 1

1University of California-Davis Davis USA2Colorado State University Ft. Collins USA

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12:15 PM - CCC6.08
3-Dimensional Micro/Nano-Structuring and Analysis of Novel SOFCs Using Focused Ion and Electron Beams

Meltem Sezen 1 Shalima Shawuti 2 Saso Sturm 3 Mehmet Ali Gulgun 2

1Sabanci University Istanbul Turkey2Sabanci University Istanbul Turkey3Jozef Stefan Institute Ljubljana Slovenia

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