2018 MRS Fall Meeting and Exhibit | Boston, Massachusetts

Symposium CM03 : In Situ/Operando Analysis of Electrochemical Materials and Interfaces

2018-11-26   Show All Abstracts

Symposium Organizers

Hao Ming Chen, National Taiwan University
Neil Dasgupta, University of Michigan
Vanessa Wood, ETH Zürich
Matthew McDowell, Georgia Institute of Technology

Symposium Support

Georgia Institute of Technology, Institute for Materials
Hitachi High Technologies America, Inc.
Joule | Cell Press
Protochips, Inc.
Toyota
University of Michigan, Department of Mechanical Engineering
CM03.01: Battery Interfaces
Session Chairs
Matthew Boebinger
Neil Dasgupta
Kelsey Hatzell
Monday PM, November 26, 2018
Hynes, Level 3, Room 300

8:15 AM - *CM03.01.01
Single Particles Cathode Material Electrochemical Properties from Micro-Pipets Methods

Janine Mauzeroll1,Malak Dayeh1,Micheal Snowden1,2,Mohammadreza Ghavidel1,2,Steen Schougaard2

McGill University1,Université du Québec à Montréal2

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8:45 AM - CM03.01.02
In Situ/Operando Soft X-Ray Spectroscopy of Interfacial Processes in Energy Materials and Catalysis

Yi-Sheng Liu1,Liang Zhang1,Jinghua Guo1

Lawrence Berkeley National Lab1

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9:00 AM - CM03.01.03
Enabling Ultrafast Interfacial Li-Transport in Layered-Oxide Cathodes

Bohua Wen1,Ping-Chun Tsai1,Menghsuan Pan1,Yet-Ming Chiang1

Massachusetts Institute of Technology1

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9:15 AM - CM03.01.04
Interfacial Studies of the Solid Electrolyte Interphase

Hans-Georg Steinrueck1,Chuntian Cao1,2,Iwnetim Abate1,2,Michael Toney1

SLAC National Accelerator Laboratory1,Stanford University2

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9:30 AM - CM03.01.05
Investigating Molecular Structures at Interface Using Nanogap Surface-Enhanced Raman Spectroscopy

Guang Yang1,Robert Sacci1,Ilia Ivanov1,Rose Ruther1,Kevin Hays1,Yiman Zhang1,Pengfei Cao1,Gabriel Veith1,Nancy Dudney1,Tomonori Saito1,Daniel Hallinan2,Jagjit Nanda1

Oak Ridge National Laboratory1,Florida State University2

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9:45 AM - CM03.01
BREAK


CM03.02: Transformations in Battery Materials
Session Chairs
Matthew Boebinger
Neil Dasgupta
Kelsey Hatzell
Monday PM, November 26, 2018
Hynes, Level 3, Room 300

10:45 AM - CM03.02.02
Visualizing Intercalation Events in Ultrathin Graphite Electrodes

Madeline Stark1,Hailey Kim1,Judy Cheng1,Scott Warren1

University of North Carolina at Chapel Hill1

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11:00 AM - CM03.02.03
Insertion and Conversion Based Electrochemical Energy Storage Systems—Complementary Insights from Ex Situ, In Situ and Operando Spectroscopy, Diffraction and Electrochemistry Studies

Amy Marschilok1,2,Kenneth Takeuchi1,Esther Takeuchi1,2

Stony Brook University1,Brookhaven National Laboratory2

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11:15 AM - CM03.02.04
In Situ Investigation of Multi-Step Lithiation of Tin Sulfide

Dong Su1,Sooyeon Hwang1,Zhenpeng Yao2,Lei Zhang3,Maosen Fu4,Kai He2,Liqiang Mai3,Chris Wolverton2

Brookhaven National Laboratory1,Northwestern University2,Wuhan University of Technology3,Northwestern Polytechnical University4

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11:30 AM - CM03.02.05
In Situ S/TEM of SnO2 Nano-Clusters for Li-Anodes

Katherine Jungjohann1,Shalini Tripathi2,3,Subrahmanyam Goriparti1,C Carter2,1,Narayanan Ravishankar3

Sandia National Laboratories1,University of Connecticut2,Indian Institute of Science3

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11:45 AM - CM03.02.06
Structural Characterization of the Atomic and Electronic Evolution of Complex Metal Oxides in High-Rate Energy Storage

Kent Griffith1,Kamila Wiaderek2,Giannantonio Cibin3,Lauren Marbella1,Clare Grey1

University of Cambridge1,Argonne National Laboratory2,Diamond Light Source3

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CM03.03: Solid-State Electrolytes I
Session Chairs
Matthew Boebinger
Katherine Jungjohann
Dong Su
Monday PM, November 26, 2018
Hynes, Level 3, Room 300

1:30 PM - *CM03.03.01
When Lithium Travels in Solid-State Disorder for Novel Device Prototypes to Store Energy, Sense the Environment or Emulate Data

Jennifer Rupp1

Massachusetts Institute of Technology1

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2:00 PM - CM03.03.02
X-Ray Tomography Studies of Ceramic Solid Electrolytes for Solid-State Battery Applications

Kelsey Hatzell1,Marm Dixit1,Fengyu Shen1

Vanderbilt University1

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2:15 PM - CM03.03.03
Multi-Modal Characterization of Li10GeP2S12 Solid Electrolyte Stability in Solid-State Lithium Metal Batteries

Andrew Davis1,Kevin Wood2,Regina Garcia-Mendez1,Kuan-Hung Chen1,Eric Kazyak1,Jeff Sakamoto1,Glenn Teeter2,Neil Dasgupta1

University of Michigan1,National Renewable Energy Laboratory2

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2:30 PM - *CM03.03.04
In Situ Scanning Electron Microscope Observations of Li Plating/Stripping Reactions on Oxide Solid Electrolytes

Munekazu Motoyama1,Takayuki Yamamoto1,Yasutoshi Iriyama1

Nagoya University1

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3:00 PM - CM03.03
BREAK


CM03.04: High Capacity Battery Electrodes
Session Chairs
Matthew Boebinger
Katherine Jungjohann
Dong Su
Monday PM, November 26, 2018
Hynes, Level 3, Room 300

3:30 PM - *CM03.04.01
Multimodal X-Ray Characterization of Operating Electrochemical Energy Storage Systems

Johanna Weker1

SLAC National Accelerator Lab1

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4:00 PM - CM03.04.02
Revealing Nanoscale Passivation and Corrosion Mechanisms of Reactive Battery Materials in Gas Environments

Yuzhang Li1,Yi Cui1

Stanford University1

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4:15 PM - CM03.04.03
Operando Characterization of Lithium Metal Plating and Stripping Using Grazing Incidence Small Angle X-Ray Scattering

Michael Toney2,Robert Kasse1,2,Natalie Geise1,2,Hans-Georg Steinrueck2

Stanford University1,SLAC National Accelerator Laboratory2

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4:30 PM - CM03.04.04
Multiscale Modeling and In Situ Visualization Analyses of Electrodeposition in Nanostructured Electrolytes

Snehashis Choudhury1,Lynden Archer1

Cornell University1

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4:45 PM - CM03.04.05
Coupling Operando Techniques for Unravelling the Electrochemical and Structural Mechanism of High-Performance Lithiated Nitrides as Negative Electrode Material for Li-Ion Batteries

Nicolas Emery1,Jean-Pierre Pereira-Ramos1

ICMPE-GESMAT UMR 71821

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2018-11-27   Show All Abstracts

Symposium Organizers

Hao Ming Chen, National Taiwan University
Neil Dasgupta, University of Michigan
Vanessa Wood, ETH Zürich
Matthew McDowell, Georgia Institute of Technology

Symposium Support

Georgia Institute of Technology, Institute for Materials
Hitachi High Technologies America, Inc.
Joule | Cell Press
Protochips, Inc.
Toyota
University of Michigan, Department of Mechanical Engineering
CM03.05: Batteries I
Session Chairs
Neil Dasgupta
Matthew McDowell
Adrian Sanchez
Tuesday AM, November 27, 2018
Hynes, Level 3, Room 300

8:15 AM - *CM03.05.01
Correlative Imaging of Electrochemical Devices Over Multiple Time and Length Scales

Paul Shearing1

University College London1

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8:45 AM - CM03.05.02
Monitoring Capacity Losses Through Operando X-Ray Diffraction in Lithium Metal Anodes

Michael Toney2,Natalie Geise1,2,Robert Kasse1,2,Hans-Georg Steinrueck2

Stanford University1,SLAC National Accelerator Laboratory2

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9:00 AM - CM03.05.03
Plan-View Operando Video Microscopy of Li Metal Anodes

Adrian Sanchez1,Kuan-Hung Chen1,Eric Kazyak1,Neil Dasgupta1

University of Michigan Ann Arbor1

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9:15 AM - CM03.05.04
In Situ/Operando Grazing Incidence Small Angle X-Ray Scattering of Model Oxide Nanostructures for Li-Ion Battery Conversion Electrodes

Jae Jin Kim1,Byeongdu Lee1,Chun Zhou2,Hyo Seon Suh2,Anil Mane1,Jeffrey Elam1,Paul Nealey2,Paul Fenter1,Tim Fister1

Argonne National Laboratory1,The University of Chicago2

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9:30 AM - CM03.05.05
Reaction with Larger Ions Avoids Fracture in a Conversion Battery Material—In Situ TEM Investigation

Matthew Boebinger1,Baolin Wang1,Marc Papakyriakou1,Shuman Xia1,Ting Zhu1,Matthew McDowell1

Georgia Institute of Technology1

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9:45 AM - CM03.05
BREAK


CM03.06: Solid and Liquid Interfaces
Session Chairs
Neil Dasgupta
Matthew McDowell
Adrian Sanchez
Tuesday PM, November 27, 2018
Hynes, Level 3, Room 300

10:15 AM - *CM03.06.01
Scanning Electrochemical Microscopy of Battery Interfaces—Versatile Imaging Using Novel Ionic Probes and Multimodal Raman Interrogation

Joaquin Rodriguez-Lopez1,Zachary Gossage1,Noah Schorr1,Jingshu Hui1,Zachary Barton1

University of Illinois at Urbana Champaign1

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10:45 AM - CM03.06.02
Cryo-Electron Microscopy for Battery Materials

Yanbin Li1,Yi Cui1

Stanford University1

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11:00 AM - *CM03.06.03
Electrochemical Interfacial Properties Revealed by Synergistically Combining Ambient Pressure XPS with Theory

Ethan Crumlin1

Lawrence Berkeley National Laboratory1

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11:45 AM - CM03.06.05
Electrified Solid/Liquid Interface Studied by Nanoelectrical and Nanoelectrochemical Atomic Force Microscopy

Zhuangqun Huang1,Peter De Wolf1,Antoine Dujardin1,2,Bede Pittenger1,Thomas Mueller1

Bruker Nano Surfaces1,Lille Centre for Infection and Immunity, CNRS UMR8204, INSERM U1019, Lille Regional Hospital University Centre, University of Lille, Institut Pasteur de Lille2

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CM03.07: Photoelectrochemistry
Session Chairs
Ethan Crumlin
Matthew McDowell
Adrian Sanchez
Tuesday PM, November 27, 2018
Hynes, Level 3, Room 300

1:30 PM - CM03.07.01
In Situ Raman Investigation of Doped Ceria Redox Mechanisms Under Solar-to-Fuel Conversion Schemes

Claire Halloran1,Alfonso Carrillo1,Eva Sediva1,2,Jennifer Rupp1

Massachusetts Institute of Technology1,ETH Zürich2

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1:45 PM - CM03.07.02
Operando Characterization of Charge Extraction Profiles in Semiconductor Photoelectrodes with Nanoscale Resolution

Gideon Segev1,Chang-Ming Jiang1,2,Gregory Zaborski1,Jason Cooper1,Francesca Maria Toma1,Ian Sharp1,2

Lawrence Berkeley National Laboratory1,Technische Universität München2

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2:00 PM - CM03.07.03
The Dynamics of Bubble Evolution on Structured Photoelectrochemical Interfaces

Zebulon Schichtl1,Hamed Mehrabi1,James Lowe1,Robert Coridan1

University of Arkansas1

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2:15 PM - CM03.07.04
Transient Absorption and Theoretical Studies of the Effect of Nitridation Time on Carrier Dynamics Of Ta3N5 Photoelectrodes for Overall Water Splitting

Kazuhiko Seki1,Dharmapura H. K. Murthy1,Yohichi Suzuki1,2,Hiroyuki Matsuzaki1,Akihiro Furube3,Zheng Wang4,Yasunobu Inoue4,Takashi Hisatomi5,Qian Wang4,Tsuyoshi Takata5,Shanshan Chen4,Kazunari Domen4

AIST1,Keio university2,Tokushima University3,Tokyo university4,Shinshu university5

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2:30 PM - CM03.07.05
Disentangling the Role of Surface Chemical Interactions on Interfacial Charge Transport at BiVO4 Photoanodes

Johanna Eichhorn1,Christoph Kastl1,Adam Schwartzberg1,Ian Sharp2,Francesca Maria Toma1

Lawrence Berkeley National Laboratory1,Technische Universität München2

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2:45 PM - CM03.07.06
Photoelectrochemical Scanning Droplet Cell Microscopy on Fe, Ni, Co Doped Tungsten Oxide Material Libraries

Achim Walter Hassel1,2,3,Junseob Lee3,1,Cezarina Mardare2,1,Andrei Mardare1,3,Jan Kollender1

Johannes Kepler Univ1,CD-Lab COMBOX2,CEST Competence Center for Electrochemical Surface Science3

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3:00 PM - CM03.07
BREAK


CM03.08: Electrocatalysis
Session Chairs
Ethan Crumlin
Matthew McDowell
Adrian Sanchez
Tuesday PM, November 27, 2018
Hynes, Level 3, Room 300

3:30 PM - *CM03.08.01
Probing Electrochemical Reactions Under Operando Condition

Bin Liu1

Nanyang Technological University1

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4:00 PM - CM03.08.02
Probing the Promotion of CO Reduction at the Cu/Electrolyte Interface Using a Combined In Situ IR Spectroscopy and Online Electrochemical Mass Spectrometry Approach

Matthias Waegele1

Boston College1

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4:15 PM - CM03.08.03
Revealing CO2 Adsorption Tunability on Metal Catalyst Surfaces

Yifan Ye1,Hao Yang2,Jin Qian2,Junko Yano1,William Goddard2,Ethan Crumlin1

Lawrence Berkeley National Lab1,California Institute of Technology2

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4:30 PM - CM03.08.04
Differential Electrochemical Mass Spectrometry for Electrocatalysis—Au-Based Systems for CO2 Reduction Case Study

Daniele Perego1,Juan Herranz1,Marie Porto1,Thomas Schmidt1

Paul Scherrer Institut1

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4:45 PM - CM03.08.05
Multimodal Operando X-ray Characterization of Electrocatalytic Interfaces for Solar Fuels Production

Walter Drisdell1,Maryam Farmand1,Alan Landers2,Christopher Hahn3

Lawrence Berkeley National Laboratory1,Stanford University2,SLAC National Accelerator Laboratory3

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CM03.09: Poster Session I: In Situ Investigation of Electrochemical Materials
Session Chairs
Neil Dasgupta
Matthew McDowell
Wednesday AM, November 28, 2018
Hynes, Level 1, Hall B

8:00 PM - CM03.09.01
The Electrochemical Study of the Interaction Between Bacterial Cytochromes and Iron Oxide Minerals

Hanyu Wang1,Alexander Johs1,Jim Browning1,Liyuan Liang1,Alan Tennant1

Oak Ridge National Lab1

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8:00 PM - CM03.09.02
Investigation of the Valence Variation of Ruthenium Oxide Nanosheet Between the Low and High Potential Regions Using In Situ XAFS

Takahiro Saida1,Fumiaki Sato1,Takahiro Maruyama1

Meijo Univ1

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8:00 PM - CM03.09.04
Effect of Coating on Lithiation in LiMn2O4

Kimberly Bassett1,Robert Warburton2,Siddharth Desphande2,Tim Fister3,Kim Ta1,Jennifer Esbenshade1,Kamila Wiaderek3,Karena Chapman3,Jeffrey Greeley2,Andrew Gewirth1

University of Illinois at Urbana-Champaign1,Purdue University2,Argonne National Laboratory3

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8:00 PM - CM03.09.06
In Situ Optical Spectroscopy During Electrochemical Coloration of WO3 Thin Films

Simon Burkhardt1,Jan Luka Dornseifer1,Alexander Günter Strack1,Matthias Elm1,Bernhard Lani-Wayda1,Peter Klar1

Justus Liebig University Giessen1

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8:00 PM - CM03.09.07
A Study of Direct Methane Oxidation at Ceria/Gas Electrochemical Interface

Yoonseok Choi1,JeongDo Yoo1,Han Gil Seo1,Hyun You Kim2,WooChul Jung1

KAIST1,Chungnam National University2

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8:00 PM - CM03.09.09
Why Does Oxide-Derived Silver Work so Well as an Electrocatalyst for CO2 Reduction? An EXAFS Study

Nienke Firet1,Marijn Blommaert1,Thomas Burdyny1,Anirudh Venugopal1,Alessandro Longo2,Wilson Smith1

Delft University of Technology1,European Synchrotron Radiation Facility2

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8:00 PM - CM03.09.10
In Situ XANES and PDF Analysis of Electrochemical Cycling of Defective δ-MnO2 Nanosheet Electrodes

Madeleine Flint1,Peng Gao1,Robert Koch1,Alec Ladonis1,Scott Misture1

Alfred University1

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8:00 PM - CM03.09.11
High-Temperature Thin-Film Calorimetry

Holger Fritze1,Hendrik Wulfmeier1,Alexander Omelcenko1

Clausthal Univ of Technology1

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8:00 PM - CM03.09.12
The Effect of Illumination on the Geometric Structure of Water Molecules on GaN(0001) Surface

Masahiro Sato1,Yuki Imazeki1,Katsushi Fujii2,Yoshiaki Nakano1,Masakazu Sugiyama1

The University of Tokyo1,RIKEN2

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8:00 PM - CM03.09.13
Charge Transfer Dynamical Processes at Graphene-Transition Metal Oxides/Electrolyte Interface—Insights from In Situ Raman Spectro-Electrochemistry

Sanju Gupta1,Sara Carrizosa1

Western Kentucky University1

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8:00 PM - CM03.09.14
Replicating Bulk Electrochemistry in Multimodal Liquid Cell Microscopy

Khim Karki1,Julio Rodriguez Manzo1,Daan Alsem1,J. Tyler Mefford2,Jungjin Park2,William Chueh2,Norman Salmon1

Hummingbird Scientific1,Stanford University2

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2018-11-28   Show All Abstracts

Symposium Organizers

Hao Ming Chen, National Taiwan University
Neil Dasgupta, University of Michigan
Vanessa Wood, ETH Zürich
Matthew McDowell, Georgia Institute of Technology

Symposium Support

Georgia Institute of Technology, Institute for Materials
Hitachi High Technologies America, Inc.
Joule | Cell Press
Protochips, Inc.
Toyota
University of Michigan, Department of Mechanical Engineering
CM03.10: Battery Materials Properties
Session Chairs
Matthew Boebinger
Matthew McDowell
Jagjit Nanda
Wednesday AM, November 28, 2018
Hynes, Level 3, Room 300

8:00 AM - CM03.10.01
In Situ Observation of Magnetic Changes During Electrochemical Reactions of FeOx/Fe Nanostructures

Jonas Zehner1,Kenny Duschek1,Ivan Soldatov1,Nicolas Perez1,Andreas Petr1,Sebastian Faehler1,Rudolf Schaefer1,Kornelius Nielsch1,Karin Leistner1

IFW Dresden1

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8:15 AM - CM03.10.02
Thermal Conductivity Changes of TiO2, V2O5, NiO, Fe2O3 and Sb During Electrochemical Cycling with Li+ Ions

Jungwoo Shin1,Sanghyeon kim1,HoonKee Park2,Ho Won Jang2,David Cahill1,Paul Braun1

University of Illinois at Urbana-Champaign1,Seoul National University2

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8:30 AM - CM03.10.03
Operando Probing of Phase Transformation in LiXTiO2 Using Electronic Conductivity and Its Applications in Neuromorphic Computing

A. Talin1,Yiyang Li1,Elliot Fuller1,Yuping He1,Sapan Agarwal1

Sandia National Laboratories1

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CM03.11: Batteries II
Session Chairs
Matthew Boebinger
Matthew McDowell
Jagjit Nanda
Wednesday PM, November 28, 2018
Hynes, Level 3, Room 300

8:45 AM - CM03.11.01
Combined TXM/Acoustic Study of Sudden Pouch Cell Expansion

Daniel Steingart1,Clement Bommier1

Princeton University1

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9:00 AM - CM03.11.02
Simultaneous Operando Measurements of the Local Temperature, State of Charge and Strain Inside a Commercial Lithium-Ion Battery Pouch Cell

Stephen Harris1,Zhili Feng2,Yang Ren3

Lawrence Berkeley National Laboratory1,Oak Ridge National Laboratory2,Argonne National Laboratory3

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9:15 AM - CM03.11.03
Interrogating Electrolyte Decomposition Reactions in Advanced Batteries with Collector-Generator Measurements and Molecular Probes

Maureen Tang1,Oliver Harris1,Sophia Lee1

Drexel University1

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9:30 AM - *CM03.11.04
Using In Situ and Operando Methods to Characterize Phase Changes in Charged Lithium Nickel Cobalt Aluminum Oxide Cathode Materials

Eric Stach1,2,Sooyeon Hwang3,Khim Karki2,Seung Min Kim4,Seongmin Bak3,Dongdong Xiao5,Noah Glachman1,Wonyoung Chang4,Kyung Yoon Chung4,Guangwen Zhou5,M. Stanley Whittingham5,Xiao-Qing Yang3,Y. Shirley Meng6

University of Pennsylvania1,Hummingbird Scientific2,Brookhaven National Laboratory3,Korea Advanced Institute of Science and Technology4,Binghamton University, The State University of New York5,University of California, San Diego6

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10:00 AM - CM03.11
BREAK


CM03.12: Solid-State Electrolytes II
Session Chairs
Matthew Boebinger
Matthew McDowell
Jagjit Nanda
Wednesday PM, November 28, 2018
Hynes, Level 3, Room 300

10:30 AM - *CM03.12.01
Probing Interfacial Charge Transfer Limitations of Sulfide Solid Electrolytes for All Solid-State Battery Applications

Y. Shirley Meng1,2

University of California, San Diego1,Sustainable Power and Energy Center (SPEC)2

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11:00 AM - CM03.12.02
Operando XPS and In Situ SAM Measurements of Solid Electrolyte Interphase Formation at Lithium/Solid Electrolyte Interfaces

Glenn Teeter1,Kevin Wood1,Andrew Davis2,K. Steirer3,Shriram Santhanagopalan1,Chunmei Ban1,Sehee Lee4,Neil Dasgupta2

National Renewable Energy Laboratory1,University of Michigan–Ann Arbor2,Colorado School of Mines3,University of Colorado Boulder4

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11:15 AM - CM03.12.03
Lithium-Electrolyte Interface Characterization in All-Solid Batteries with Operando Electron and X-Ray Microscopies

Natalie Seitzman1,Harvey Guthrey2,Johanna Weker3,Heather Platt4,Mowafak Al-Jassim2,Svitlana Pylypenko1

Colorado School of Mines1,National Renewable Energy Laboratory2,SLAC National Accelerator Laboratory3,Solid Power, Inc.4

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11:30 AM - *CM03.12.04
Elucidating Ion Transport and Charge Transfer Behavior at Solid-Solid Interfaces via STEM

Miaofang Chi1

Oak Ridge National Laboratory1

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CM03.13: Battery Interfaces and Ion Insertion
Session Chairs
Matthew Boebinger
Miaofang Chi
Stephen Harris
Wednesday PM, November 28, 2018
Hynes, Level 3, Room 300

1:30 PM - *CM03.13.01
X-Ray and Optical Spectroscopy and Imaging of the Electrode/Electrolyte Interface on Intermetallic Anodes

Robert Kostecki1,Philip Ross1,Hans Bechtel1,Jinghua Guo1,Liang Zhang1,Atetegeb Haregewoin1,Ivana Hasa1

Lawrence Berkeley National Lab1

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2:00 PM - *CM03.13.02
Understanding the Many Length Scales of Ion Insertion Solids

William Chueh1

Stanford University1

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