April 22 - 26, 2024
Seattle, Washington
May 7 - 9, 2024 (Virtual)

Event Supporters

2024 MRS Spring Meeting
CH04.04.02

In-Situ/Operando Bragg Coherent X-Ray Diffraction Imaging for Visualization of Nanoscale Structural Evolution

When and Where

Apr 24, 2024
8:15am - 8:30am
Room 443, Level 4, Summit

Presenter(s)

Co-Author(s)

Wonsuk Cha1

Argonne National Laboratory1

Abstract

Wonsuk Cha1

Argonne National Laboratory1
In the last two decades, Bragg Coherent X-ray Diffraction Imaging (BCDI) has become a powerful non-destructive 3D characterization tool for features in nanoscale [1]. Because of unique sensitivity to lattice, BCDI has been employed on various nano-scaled materials such as metal, metal oxide, and mineral, to reveal 3D map of lattice distortion and strain distribution. Adding in-situ and operando approaches to BCDI enables to address scientific questions on physics, chemistry, and materials science in recent years.<br/>In this talk, I will introduce current state-of-art of BCDI and recent experimental results on in-situ and operando BCDI. Annealing effect on gold grains on thin films [2], relaxation of strain inside quantum materials such as nanodiamond and silicon carbide [3, 4]. Strain and defect in battery materials [5] and in catalysts [6] will be discussed. In addition, some estimates of BCDI in the near future will be discussed.<br/><br/>[1] M. A. Pfeifer, et al., Nature 442, 63 (2006).<br/>[2] A. Yau, et al., Science 356, 739 (2017).<br/>[3] S. O. Hruszkewycz, et al., APL Mater. 5, 026105 (2017).<br/>[4] S. O. Hruszkewycz, et al., Phys. Rev. Mater. 2, 086001 (2018).<br/>[5] A. Singer, et al., Nat. Energy 3, 641 (2018).<br/>[6] D. Kim, et al., Nature Communications, 9, 3422 (2018).

Keywords

in situ | nanostructure | operando

Symposium Organizers

Yuzi Liu, Argonne National Laboratory
Michelle Mejía, Dow Chemical Co
Yang Yang, Brookhaven National Laboratory
Xingchen Ye, Indiana University

Session Chairs

Tao Sun
Tao Zhou

In this Session