December 1 - 6, 2024
Boston, Massachusetts

Event Supporters

2024 MRS Fall Meeting & Exhibit
SB13.06.02

Characterization of Channel Structures Observed in the Radiation-Induced Dielectric Breakdown of Polymethyl Methacrylate for Space Applications

When and Where

Dec 4, 2024
2:15pm - 2:30pm
Hynes, Level 3, Room 308

Presenter(s)

Co-Author(s)

Raphael Rose1,Bryson Clifford1,Karen Wiratan1,Noah Hoppis1,Kathryn Sturge1,Holly Wilson1,Carolyn Chun1,John Cumings1,Timothy Koeth1

University of Maryland1

Abstract

Raphael Rose1,Bryson Clifford1,Karen Wiratan1,Noah Hoppis1,Kathryn Sturge1,Holly Wilson1,Carolyn Chun1,John Cumings1,Timothy Koeth1

University of Maryland1
Dielectric breakdown due to solar radiation poses a significant problem for polymers in space. This type of component failure can be modeled in bulk dielectric materials, such as polymethyl methacrylate (PMMA). We irradiate the PMMA with an electron accelerator to accumulate space charge within the bulk, this we discharge by mechanical insult to force an electrical breakdown. This process forms permanent dendritic breakdown patterns, colloquially known as electrical trees. Here we study and categorize these trees using optical and electron microscopy by computer vision, and X-ray computed tomography.<br/> <br/>We investigate the various types of discharge. Other authors [1,2] have categorized the discharge channel structures into branch and bush types by their morphology. However, our analysis provides the first characterization of novel discharge channel types only observed in radiation-based dielectric breakdown [3]. We provide a structural description including a heuristic analysis and channel diameter measurements.<br/> <br/>We confirm the presence of branch and bush discharge structures and characterize a novel discharge structure and transition channel type, both of which suggest gaps in the present understanding of the physical processes at play.<br/> <br/>Acknowledgements:<br/>This work is supported by the Defense Advanced Research Projects Agency<br/> <br/>References:<br/>1. R. Schurch, S. M. Rowland, R. S. Bradley and P. J. Withers, in IEEE Transactions on Dielectrics and Electrical Insulation, vol. 21, no. 1, pp. 53-63, 2014, doi: 10.1109/TDEI.2013.003911.<br/>2. L. A. Dissado and J. C. Fothergill, in “Electrical Degradation and Breakdown in Polymers,” ed. Peter Peregrinus Ltd., (London, UK) 1992.<br/>3. K. Sturge, et al, in “Dynamics of High-Speed Electrical Tree Growth in Electron-Irradiated Polymethyl Methacrylate,” Science, (in press).

Keywords

electron irradiation | scanning electron microscopy (SEM) | x-ray tomography

Symposium Organizers

Ahmad Kirmani, Rochester Institute of Technology
Felix Lang, Universität Potsdam
Joseph Luther, National Renewable Energy Laboratory
Ian Sellers, University at Buffalo, The State University of New York

Symposium Support

Bronze
APL Energy
Nextron Corporation

Session Chairs

Ian Sellers
Michael Short

In this Session